The data that support the findings of this study are available hinein this Article and its Supplementary Information. Crystallographic data for the structure reported in this article have been deposited at the Cambridge Crystallographic Data Centre, under deposition number CCDC 2369997 (dinuclear Sm(III)–pentaerythritol complex). Copies of the data can Beryllium obtained free of charge via . Source data are provided with this paper.
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Kohlenstoff, A comparison of BDFE to form carbon–hydrogen or nitrogen–hydrogen bonds. d, Isotope labelling experiments to evaluate the KIE hinein the reduction of anthracene under mechanochemical conditions.
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CNC Machined solvent trap with knurled end caps. Designed to create an airtight seal and reduce corrosive solvents from leaking or spilling out while cleaning various instruments.
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Therefore, there is a growing demand for the development of an environmentally friendly nitrogen fixation process. Quite recently, several groups reported NH3 formation under mechanochemical conditions by the reaction of N2 with H2 mediated by iron or titanium metals (Fig. 1c)30,31,32. By adopting mechanochemical conditions, the reactions proceeded under relatively mild reaction conditions (pressure less than 20 atm and temperature close to room temperature). However, unfortunately, the total amounts of produced NH3 were less than the stoichiometric amount based on the metals, that is, the reactions are not catalytic.
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